Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
m-Formylbenzonitrile → [3-(Aminomethyl)phenyl]methanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | m-Formylbenzonitrile | HCID 90670 | — |
| 반응물 | [3,5-Bis(benzyloxy)benzyl]amine hydrochloride | HCID 15505554 | — |
| 생성물 | [3-(Aminomethyl)phenyl]methanol | HCID 21880609 | 66% |
반응 단계
This compound was prepared by reduction of 3-cyanobenzaldehyde according to the procedure described in preparation of 3,5-dibenzyloxybenzylamine. Yield was 66%: 1H NMR (Acetone-d6, 500 MHz) δ 7.32 (s, 1H), 7.23 (dd, 1H, J=7.6 and 7.0), 7.19, complex, 2H), 4.59 (s, 2H), 4.40 (s, 2H), 4.10 (br, 1H), 1.96 (br, 1H), 1.88 (br, 1H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07427608B2 |
| 출처 데이터셋 | uspto-grants-2008_09 |
| ORD ID | ord-b76b6ae21fe944ad8b04497ca70cb28e |
| 출처 메모 | uspto-grants-2008_09 |