Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triphenylphosphine → 3-Amino-1-(diphenylmethyl)azetidine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triphenylphosphine | HCID 11776 | — |
| 반응물 | 3-Azido-1-benzhydrylazetidine | HCID 15512652 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 3-Amino-1-(diphenylmethyl)azetidine | HCID 5744546 | — |
반응 단계
A solution of 10 (5.7 g, 21.6 mmol), triphenylphosphine (11.3 g, 43 mmol) and water (5 ml) was heated to reflux for 24 hours. After cooling to room temperature the solvent was removed in vacuo and the residue purified by chromatography on silica gel (90:9:1 CHCl3:MeOH:NH4OH).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06214832B1 |
| 출처 데이터셋 | uspto-grants-2001_04 |
| ORD ID | ord-f60b66a271f9493a9e18eb43c1e0e25d |
| 출처 메모 | uspto-grants-2001_04 |