Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Isopropanol → Baccatin III isopropanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Isopropanol | HCID 3776 | — |
| 반응물 | Hexane | HCID 8058 | — |
| 반응물 | Baccatin Iii | HCID 65366 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Baccatin III isopropanol | HCID 86756610 | — |
반응 단계
Baccatin III (100 mg, 0.17 mmol) was dissolved in dichloromethane (4 mL). Isopropanol was added (130 uL, 1000%), and the resulting solution was allowed to stir for 1 h. Hexane was added to the cloud point, and crystallization began. The baccatin III, 2-propanol complex (85 mg, 77%) was collected by filtration.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06215000B1 |
| 출처 데이터셋 | uspto-grants-2001_04 |
| ORD ID | ord-faa71747695648ada0aeab7e1000d413 |
| 출처 메모 | uspto-grants-2001_04 |