Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ioxynic acid → 2,6-Diiodo-4-(8-phenyloctylcarbamoyl)phenol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ioxynic acid | HCID 12065 | — |
| 반응물 | 8-Phenyloctan-1-amine | HCID 145556 | — |
| 생성물 | 2,6-Diiodo-4-(8-phenyloctylcarbamoyl)phenol | HCID 22237559 | — |
반응 단계
The title compound was prepared as a solid (0.718 g, 66%) from 3,5-diiodo-4-hydroxybenzoic acid using 8-phenyloctylamine and a procedure similar to step 2 of Example 93; 1H NMR (DMSO-d6) δ1.17-1.36 (m, 8H), 1.41-1.61 (m, 4H), 2.48-2.60 (m, 2H), 3.20 (dd, J=5.9, 8.8 Hz, 2H), 7.10-7.21 (m, 3H), 7.21-7.30 (m, 2H), 8.21 (s, 2H), 8.40 (t, J=4.4 Hz, 1H), 10.06 (s, 1H); mass spectrum [(+) ESI], m/z 578 (M +H)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06214877B1 |
| 출처 데이터셋 | uspto-grants-2001_04 |
| ORD ID | ord-f11b309d33c0464e85088f9906c90eb6 |
| 출처 메모 | uspto-grants-2001_04 |