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llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
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HCID 20645779, 화합물 → HCID 20645780, 화합물

HRID 324153
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인쇄 미리보기

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HRID 324153 반응식
[CH3:1][C@H:2]([C:11]([O:13][C:14]1[CH:19]=[CH:18][C:17]([O:20]CC2C=CC=CC=2)=[CH:16][CH:15]=1)=[O:12])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]>[Pd].C(OCC)(=O)C>[CH3:1][C@H:2]([C:11]([O:13][C:14]1[CH:19]=[CH:18][C:17]([OH:20])=[CH:16][CH:15]=1)=[O:12])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 1

HCID 20645779HCID 20645779, 화합물

생성물 1

HCID 20645780HCID 20645780, 화합물수율 88.2%

시약·촉매·용매 2

HCID 23938Palladium촉매HCID 8857Ethyl Acetate용매

실험 절차

{circle around (2)}: A mixture comprising 3.0 g of (S)-4-(1′-methylnonylcarbonyloxy)-1-benzyloxybenzene, 0.3 g of palladium/carbon and 20 g of ethyl acetate was stirred for 6 hours under hydrogen atmosphere. Then, palladium/carbon was filtered off, followed by distilling off ethyl acetate from the filtrate, whereby 2.0 g of (S)-4-(1′-methylnonylcarbonyloxy)phenol was obtained in the form of a colorless oily substance.

후처리

  1. filtrationThen, palladium/carbon was filtered off
  2. distillationby distilling off ethyl acetate from the filtrate

출처 및 근거

ORD 기록
ord-ea48f83569154337a59b3c5ef730f386
출처 데이터셋
uspto-grants-2001_04
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US06217793B1

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