Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → Acridine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Isatin | HCID 7054 | — |
| 용매 | Water | HCID 962 | — |
| 용매 | Potassium Hydroxide | HCID 14797 | — |
| 생성물 | Acridine | HCID 9215 | — |
반응 단계
The isatin product was refluxed in 110 mL of 10% KOH solution in water over night. The dark green mixture was cooled and acidified with 400 mL of 1:1 ice/5 M HCl. The solid was washed with water and air-dried yielding the acridine acid. 1H NMR (DMSO-d6) δ 7.81-7.94 (m, 4H), 8.31-8.36 (m, 2H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06218137B1 |
| 출처 데이터셋 | uspto-grants-2001_04 |
| ORD ID | ord-899d982ee2cd4e77a93c91ee5f87c025 |
| 출처 메모 | uspto-grants-2001_04 |