Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → 1-Chloro-4-((3-chloro-4-methoxybenzyl)amino)-6-phthalazinecarbonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | 3-Chloro-4-methoxybenzylamine | HCID 738038 | — |
| 반응물 | 1,4-Dichlorophthalazine-6-carbonitrile | HCID 10656738 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | 1-Chloro-4-((3-chloro-4-methoxybenzyl)amino)-6-phthalazinecarbonitrile | HCID 10451065 | — |
반응 단계
6-Cyano-1,4-dichlorophthalazine (66.2 g) prepared in Preparative Example 3 and 3-chloro-4-methoxybenzylamine (92 g) were suspended in 1200 ml of tetrahydrofuran, followed by the addition of 250 ml of triethylamine. The obtained mixture was heated under reflux for 6 hours.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06218392B1 |
| 출처 데이터셋 | uspto-grants-2001_04 |
| ORD ID | ord-843c0b85ff1a49c49843a540fac71dcd |
| 출처 메모 | uspto-grants-2001_04 |