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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 32475생성일: 2026년 10월 24일

HCID 178474238, 화합물 → HCID 178507147, 화합물

https://huagongshe.com/ko/reaction/32475

반응식

참여 물질

역할이름HCID투입량
반응물HCID 178474238HCID 178474238—
용매EthanolHCID 702—
용매WaterHCID 962—
용매Potassium HydroxideHCID 14797—
생성물HCID 178507147HCID 17850714757.7%

반응 조건

온도60 °C

반응 단계

Compound 3-(4-acetamidophenyl)-4-aminofuro[2,3-d]pyrimidine 8 (242 mg) was dissolved in 2 M potassium hydroxide in the mixture of EtOH (16 mL) and water (4 mL). The mixture was heated (60° C.) for 24 h then concentrated in vacuo. Residual oil was triturated with cold water (6 mL) to give precipitation, which was filtrated, washed with water, and dried under the reduced pressure. The compound 9 (118 mg) as pale orange colored was obtained. MS(ES) m/e 227M+H].

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07427623B2
출처 데이터셋uspto-grants-2008_09
ORD IDord-f06b98cc45974b1297cfbef9da28bc0b
출처 메모uspto-grants-2008_09