Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Thiophen-2-ylprop-2-enoic acid → 3-(2-Thienyl)propanoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Thiophen-2-ylprop-2-enoic acid | HCID 92868 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 3-(2-Thienyl)propanoic acid | HCID 703169 | 77.6% |
반응 단계
To a solution of 3-(2-thienyl)acrylic acid (7 g) in ethanol was added 5% palladium on carbon and the mixture was hydrogenated at 50 psi in a Parr apparatus. The catalyst was filtered off and the solvent was removed by evaporation to yield the title compound (5.5 g) as an oil. Electrospray MS m/z 155 [M−H]+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06218538B1 |
| 출처 데이터셋 | uspto-grants-2001_04 |
| ORD ID | ord-1d78723a0ed54ea097bab6291d5bbe04 |
| 출처 메모 | uspto-grants-2001_04 |