Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonium Hydroxide → Diethyl 2,6-diisopropyl-4-(2-iodophenyl)pyridine-3,5-dicarboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonium Hydroxide | HCID 14923 | — |
| 반응물 | Ethyl isobutyrylacetate | HCID 81583 | — |
| 반응물 | 2-Iodobenzaldehyde | HCID 643439 | — |
| 생성물 | Diethyl 2,6-diisopropyl-4-(2-iodophenyl)pyridine-3,5-dicarboxylate | HCID 22005000 | — |
반응 단계
Prepared from 2-iodobenzaldehyde, ethyl isobutyrylacetate and concentrated ammonium hydroxide by the procedures described in Example 125, Steps A-B. 1H NMR (300 MHz, CDCl3): δ 0.94 (t, J=7.0 Hz, 6 H), 1.30 (d, J=6.6 Hz, 6 H), 1.34 (d, J=6.6 Hz, 6 H), 3.19 (septet, J=6.6 Hz, 2 H), 4.0 (q, J=7.0 Hz, 4 H), 7.0-7.40 (m, 3 H), 7.85 (m, 1 H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06218431B1 |
| 출처 데이터셋 | uspto-grants-2001_04 |
| ORD ID | ord-83468a8fac5d4acab7545d0ef661031c |
| 출처 메모 | uspto-grants-2001_04 |