Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
alpha-Tocopherol → HCID 86756642, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | alpha-Tocopherol | HCID 14985 | — |
| 반응물 | Benzoyl chloride, 4-amino- | HCID 177720 | — |
| 촉매 | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | HCID 86756642 | HCID 86756642 | 68% |
반응 단계
The reaction of alpha-tocopherol with 4-aminobenzoic acid chloride was carried out in the same manner with Example I, except that 10 mol % of 4-(dimethylamino)pyridine was added together with pyridine. This reaction was confirmed to proceed in a similar pattern to that of Example I as measured by thin layer chromatography. The remaining processes of Example I were repeated to produce alpha-tocopherol 4-aminobenzoate (0.61 g, yield 68%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06222051B1 |
| 출처 데이터셋 | uspto-grants-2001_04 |
| ORD ID | ord-84a2330b294a46d5b04e558ac57f83de |
| 출처 메모 | uspto-grants-2001_04 |