2-Ethylbutyraldehyde → 3,7-Diethyl-5-azanona-3,5-diene

HRID 325979

반응식

HRID 325979 반응식
[OH-].[NH4+:2].[CH2:3]([CH:5]([CH2:8][CH3:9])[CH:6]=O)[CH3:4]>>[CH2:3]([C:5](=[CH:6][N:2]=[CH:6][CH:5]([CH2:8][CH3:9])[CH2:3][CH3:4])[CH2:8][CH3:9])[CH3:4]

참가 물질

3

반응물 2

HCID 73592-EthylbutyraldehydeHCID 14923Ammonium Hydroxide

생성물 1

HCID 124134703,7-Diethyl-5-azanona-3,5-diene수율 76.5%

실험 절차

To a sample of 250 grams of 28% ammonium hydroxide was added 215 grams of 2-ethylbutyraldehyde and the heterogeneous mixture was stirred for 18 hours at ambient temperature. The resulting organic layer was separated, and after drying, slowly distilled at atmospheric pressure to yield 148.8 grams of 3,7-diethyl-5-azanona-3,5-diene.

후처리

  1. customThe resulting organic layer was separated
  2. customafter drying
  3. distillationslowly distilled at atmospheric pressure

출처 및 근거

ORD 기록
ord-7485e4e1d9c24c839b4ca499287abe82
출처 데이터셋
uspto-grants-1984_04
특허 번호
US04443609

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