Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzyl Alcohol → Benzyl 3-oxo-5-phenylpentanoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzyl Alcohol | HCID 244 | — |
| 반응물 | Ethyl 3-oxo-5-phenylpentanoate | HCID 61162 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Benzyl 3-oxo-5-phenylpentanoate | HCID 13055807 | — |
반응 단계
Ethyl 3-oxo-5-phenylpentanoate (64.2 g, 0.29 mole) was heated between 190° and 210° C. under nitrogen with benzyl alcohol (28.9 ml, 0.28 mole) for 6 hours, the ethanol formed being distilled out of the reaction mixture. The resulting pale yellow oil was essentially pure product, slightly contaminated by starting materials, n.m.r. δ(CCl4) 7.23 (5H, s), 7.06 (5H, s), 5.03 (2H, s), 3.23 (2H, s) and 2.73 (4H, s).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04444981 |
| 출처 데이터셋 | uspto-grants-1984_04 |
| ORD ID | ord-f813d5d350fc4144b00499e53ec2a0bc |
| 출처 메모 | uspto-grants-1984_04 |