Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
6-Hydroxymethylquinoline → 6-Quinolinecarbaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 6-Hydroxymethylquinoline | HCID 1514385 | — |
| 촉매 | HCID 178418406 | HCID 178418406 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | 6-Quinolinecarbaldehyde | HCID 765653 | 82.7% |
반응 단계
A mixture of 34 parts of 6-quinolinemethanol, 70 parts of manganese(IV)oxide and 300 parts of trichloromethane was stirred for 24 hours at room temperature. The reaction mixture was filtered over diatomaceous earth and the filtrate was evaporated, yielding 27.7 parts (82.7%) of 6-quinolinecarboxaldehyde; mp. 72° C. (interm. 16).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05268380 |
| 출처 데이터셋 | uspto-grants-1993_12 |
| ORD ID | ord-f0636ddc50f9408ab8832b5a92269345 |
| 출처 메모 | uspto-grants-1993_12 |