1-Propanone, 3-(dimethylamino)-1-phenyl-, hydrochloride (1:1) → 3-(Dimethylamino)-1-phenyl-1-propanone
반응식
Cl.[CH3:2][N:3]([CH3:14])[CH2:4][CH2:5][C:6]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)=[O:7].C(=O)(O)[O-].[Na+]>ClCCl>[CH3:14][N:3]([CH3:2])[CH2:4][CH2:5][C:6]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)=[O:7]참가 물질
4
실험 절차
3-Dimethylaminopropiophenone hydrochloride (20 g) was treated with aqueous sodium bicarbonate solution in dichloromethane. The layers were separated and the organic phase was dried over anhydrous magnesium sulfate, filtered, and the filtrate was evaporated to provide 15.8 g of 3-dimethylaminopropiophenone.
후처리
- customThe layers were separated
- dry with materialthe organic phase was dried over anhydrous magnesium sulfate
- filtrationfiltered
- customthe filtrate was evaporated
출처 및 근거
- ORD 기록
- ord-8405d6c06e7a480280c47c4f322f1fd8
- 출처 데이터셋
- uspto-grants-1993_12
- 특허 번호
- US05268468
반응 노트
불러오는 중…