참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Carbamic acid, ethyl ester | HCID 5641 | — |
| 반응물 | 2-Ethylhexyl glycidyl ether | HCID 17162 | — |
| 반응물 | Di-n-butyldilauryltin | HCID 9809426 | — |
| 촉매 | N,N-Dimethylbenzylamine | HCID 7681 | — |
| 생성물 | 5-(2-Ethylhexyl) oxymethyl-2-oxazolidinone | HCID 67684775 | 88% |
반응 단계
8.9 g (0.10 mole) of ethyl carbamate was dissolved in 18.6 g (0.10 mole) of 2-ethylhexyl glycidyl ether. After adding 0.41 g of N, N-dimethylbenzylamine and 0 63 g of di-n-butyltin dilaurate, the solution was heated at 160° C. for 1 hour while blowing nitrogen gas into the reaction mixture. The product was distilled under reduced pressure to give 20.0 g (88% of theory) of 5-(2-ethylhexyl) oxymethyl-2-oxazolidinone.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05268484 |
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| 출처 데이터셋 | uspto-grants-1993_12 |
|---|
| ORD ID | ord-c388f809cda045e386d237f8b7d3cc00 |
|---|
| 출처 메모 | uspto-grants-1993_12 |
|---|
