참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Calcium Acetate | HCID 6116 | — |
| 반응물 | 3-(1-Dodecen-1-yl)dihydro-2,5-furandione | HCID 32933 | — |
| 용매 | Water | HCID 962 | — |
| 용매 | Isopropanol | HCID 3776 | — |
| 생성물 | Calcium dodecenyl succinate | HCID 86747412 | 113.2% |
반응 단계
A solution of 313.5 g (1.98 mol) calcium acetate in 1000 ml water was added to a solution of 570 g (1.98 mol) dodecenyl succinic anhydride in 1000 ml isopropanol. The mixture was then heated to 90° C., left at that temperature for 1.5 h and then concentrated in a water jet vacuum. The residue was dried in vacuo in a drying cabinet at 100° C. 680 g of the calcium soap were obtained in the form of a colorless powder.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05271855 |
|---|
| 출처 데이터셋 | uspto-grants-1993_12 |
|---|
| ORD ID | ord-93f2ffbeba514eb389fbfa7f33845a47 |
|---|
| 출처 메모 | uspto-grants-1993_12 |
|---|
