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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 327089생성일: 2026년 10월 25일

2-Butanamine, 3,3-dimethyl- → N-cyano-N'-(1,2,2-trimethylpropyl)-2-pyridinecarboximidamide

https://huagongshe.com/reaction/327089

반응식

참여 물질

역할이름HCID투입량
반응물2-Butanamine, 3,3-dimethyl-HCID 520907—
반응물2-Pyridinecarboximidic acid, N-cyano-, methyl esterHCID 10012189—
용매MethanolHCID 887—
생성물N-cyano-N'-(1,2,2-trimethylpropyl)-2-pyridinecarboximidamideHCID 1973449693.5%

반응 단계

Methyl N-cyano-2-pyridinecarboximidate (0.50 g, 3.1 mmol) was dissolved in methanol (10 ml), 1,2,2-trimethylpropylamine (0.34 g, 3.4 mmol) was added, and the resulting mixture was stirred at room temperature for 30 minutes. After the reaction was completed, the reaction solution was concentrated under reduced pressure, and the residue thus obtained was crystallized from dichloromethane diethyl ether to give the title compound (0.67 g, 2.9 mmol, yield: 92%) as colorless needles.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05272164
출처 데이터셋uspto-grants-1993_12
ORD IDord-e0611a07757e4edf98cf6e1d81423ac9
출처 메모uspto-grants-1993_12