Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Carbon Dioxide → psi-Pelletierine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Carbon Dioxide | HCID 280 | — |
| 반응물 | Glutaraldehyde | HCID 3485 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Sodium Phosphate, Dibasic | HCID 24203 | — |
| 반응물 | Acetonedicarboxylic acid | HCID 68328 | — |
| 반응물 | Methylamine hydrochloride | HCID 6364545 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | psi-Pelletierine | HCID 11096 | — |
반응 단계
A 5-liter 3-necked flask was charged with 140 grams of 50% aqueous glutaric dialdehyde (Aldrich, 0.7 moles), 630 ml of water and 70.7 grams of CH3NH2.HCl (1.036 moles) which was first dissolved in 700 ml of water, 116.6 grams of acetonedicarboxylic acid (0.8 moles) which had been dissolved in 1162 ml of water, and a solution of 123.2 sodium phosphate dibasic and 10.22 grams of NaOH dissolved in 280 ml of water. The heterogeneous orange solution was stirred at room temperature for 24 hours during which time the evolution of CO2 (g) was noted.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05273736 |
| 출처 데이터셋 | uspto-grants-1993_12 |
| ORD ID | ord-f3b71019fdc74000bf0b9e63f0c756c0 |
| 출처 메모 | uspto-grants-1993_12 |