Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
11-Bromoundecanoic acid → Undecanoyl chloride, 11-bromo-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 11-Bromoundecanoic acid | HCID 17812 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 생성물 | Undecanoyl chloride, 11-bromo- | HCID 85202 | — |
반응 단계
11-Bromoundecanoic acid (400 g) was added to thionyl chloride (600 ml) and the solution heated at 80° for 0.5 hour. The thionyl chloride was distilled off and the dark oily residue distilled in vacuo to give 11-bromoundecanoyl chloride, b.p. 144°, 0.7 mm Hg, (346.8 g, 81%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05273740 |
| 출처 데이터셋 | uspto-grants-1993_12 |
| ORD ID | ord-6cf0c1ec3405470791493e943ea7bff2 |
| 출처 메모 | uspto-grants-1993_12 |