참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Ammonia | HCID 222 | — |
| 반응물 | 2,6-Dichloro-3-nitrotoluene | HCID 97155 | — |
| 생성물 | 3-Chloro-2-methyl-6-nitroaniline | HCID 12953020 | 76% |
반응 단계
A suspension of 2,6-dichloro-3-nitrotoluene (6.0 g, 29 mmol) in 50% methanolic ammonia (60 mL) was stirred at 130° C. (340 lb pressure) for 18 hours. The autoclave was cooled to -30° C., opened, and the precipitate was filtered off and washed with methanol to give 4.14 g (76%) of 3-chloro-2-methyl-6-nitrobenzenamine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05273975 |
|---|
| 출처 데이터셋 | uspto-grants-1993_12 |
|---|
| ORD ID | ord-6a783ee54f534c5382fab3da4c85a8fe |
|---|
| 출처 메모 | uspto-grants-1993_12 |
|---|
