2-(2,4-Dichlorophenoxy)ethanol → 2-(2,4-Dichlorophenoxy)ethanol sulfamate

HRID 327678

반응식

HRID 327678 반응식
[S:1](Cl)(=[O:4])(=[O:3])[NH2:2].[Cl:6][C:7]1[CH:16]=[C:15]([Cl:17])[CH:14]=[CH:13][C:8]=1[O:9][CH2:10][CH2:11][OH:12]>>[S:1]([O:12][CH2:11][CH2:10][O:9][C:8]1[CH:13]=[CH:14][C:15]([Cl:17])=[CH:16][C:7]=1[Cl:6])(=[O:4])(=[O:3])[NH2:2]

참가 물질

3

반응물 2

HCID 84442-(2,4-Dichlorophenoxy)ethanolHCID 24499Chlorosulfamic acid

생성물 1

HCID 191086892-(2,4-Dichlorophenoxy)ethanol sulfamate

실험 절차

The title compound was prepared by the procedures of Example 33 from sulfamoyl chloride and 2-(2,4-dichlorophenoxy)ethanol. The viscous oil obtained solidified and was recrystallized from isopropyl ether to give the solid title compound, mp 75°-77° C., in 35% yield.

후처리

  1. customThe viscous oil obtained solidified
  2. customwas recrystallized from isopropyl ether

출처 및 근거

ORD 기록
ord-1dee74034a374557bd1fb843cefa570e
출처 데이터셋
uspto-grants-1993_12
특허 번호
US05273993

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