Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic acid, 2-(triphenylphosphoranylidene)-, methyl ester → (E)-3-[3-[[5-(Acetyloxy)pentyl]oxy]phenyl]-2-propenoic Acid Methyl Ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic acid, 2-(triphenylphosphoranylidene)-, methyl ester | HCID 17453 | — |
| 반응물 | 3-[[5-(Acetyloxy)pentyl]oxy]benzaldehyde | HCID 19922110 | — |
| 생성물 | (E)-3-[3-[[5-(Acetyloxy)pentyl]oxy]phenyl]-2-propenoic Acid Methyl Ester | HCID 67780031 | 80% |
반응 단계
Using the procedure of example 28, the title compound was prepared in 80% yield, from 2.6 g (10.4 mmol) of 3-[[5-(acetyloxy)pentyl]oxy]benzaldehyde and 4.0 g (12 mmol) of methyl (triphenylphosphoranylidene)acetate, as a colorless solid, mp 65°-67° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05273999 |
| 출처 데이터셋 | uspto-grants-1993_12 |
| ORD ID | ord-c8004816dd8c4c1d97d0f74f3500c462 |
| 출처 메모 | uspto-grants-1993_12 |