Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Aceton-methanol → 3-dimethylamino-11-methyl-1,3,4,14b-tetrahydro-2H-pyridino [1,2-d]-dibenzo[b,f](1,4)-oxazepine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Aceton-methanol | HCID 21894497 | — |
| 반응물 | 3-dimethylamino-7-trifluoromethyl-1,3,4,14b-tetrahydro-2H-pyridino[1,2-d]-dibenzo[b,f](1,4)-thiazepine | HCID 70637428 | — |
| 생성물 | 3-dimethylamino-11-methyl-1,3,4,14b-tetrahydro-2H-pyridino [1,2-d]-dibenzo[b,f](1,4)-oxazepine | HCID 70637876 | — |
반응 단계
Rf in methanol:acetone (8:2) = 0.20 (equatorial). 3-dimethylamino-7-trifluoromethyl-1,3,4,14b-tetrahydro-2H-pyridino[ 1,2-d]-dibenzo[b,f](1,4)-thiazepine:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04016161 |
| 출처 데이터셋 | uspto-grants-1977_04 |
| ORD ID | ord-aefcbfa6dd4247baacbf836c92cfd0f5 |
| 출처 메모 | uspto-grants-1977_04 |