Acrylonitrile → 3-[(3-Hydroxypropyl)amino]propanenitrile

HRID 328182노트

반응식

HRID 328182 반응식
[NH2:1][CH2:2][CH2:3][CH2:4][OH:5].[C:6](#[N:9])[CH:7]=[CH2:8]>>[C:6]([CH2:7][CH2:8][NH:1][CH2:2][CH2:3][CH2:4][OH:5])#[N:9]

참가 물질

3

반응물 2

HCID 7855AcrylonitrileHCID 90863-Amino-1-propanol

생성물 1

HCID 135569403-[(3-Hydroxypropyl)amino]propanenitrile

실험 절차

A solution of 75 g. (1 mole) of 3-aminopropanol is stirred while 54 g. (1 mole) of acrylonitrile is added dropwise. After being allowed to stand at room temperature for several hours and preferably overnight, the reaction mixture is concentrated under reduced pressure at 50° yielding 3-(2-cyanoethyl)aminopropanol.

후처리

  1. concentrationthe reaction mixture is concentrated under reduced pressure at 50°

출처 및 근거

ORD 기록
ord-ec213696efae4142b407e4af2116f5ac
출처 데이터셋
uspto-grants-1977_04
특허 번호
US04016209

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