Lauric acid diethanolamide → 2-[Dodecanoyl-[2-(furan-2-carbonyloxy)ethyl]amino]ethyl furan-2-carboxylate

HRID 328426노트

반응식

HRID 328426 반응식
[OH:1][CH2:2][CH2:3][N:4]([CH2:18][CH2:19][OH:20])[C:5](=[O:17])[CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].[O:21]1[CH:25]=[CH:24][CH:23]=[C:22]1[C:26](Cl)=[O:27]>>[O:21]1[CH:25]=[CH:24][CH:23]=[C:22]1[C:26]([O:1][CH2:2][CH2:3][N:4]([CH2:18][CH2:19][O:20][C:26]([C:22]1[O:21][CH:25]=[CH:24][CH:23]=1)=[O:27])[C:5](=[O:17])[CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16])=[O:27]

참가 물질

3

반응물 2

HCID 8430Lauric acid diethanolamideHCID 682422-Furancarbonyl chloride

생성물 1

HCID 3216912-[Dodecanoyl-[2-(furan-2-carbonyloxy)ethyl]amino]ethyl furan-2-carboxylate

실험 절차

N,N-bis(2-furoyloxyethyl)lauramide was prepared by the procedure of example 1 from 28 gms. (0.1 mole) of N,N-bis(2-hydroxyethyl)lauramide and 26 gms. (0.2 mole) of furoyl chloride. The structure of the final product was characterized on the basis of IR and NMR spectral analyses as described in example 1.

후처리

  1. customN,N-bis(2-furoyloxyethyl)lauramide was prepared by the procedure of example 1 from 28 gms

출처 및 근거

ORD 기록
ord-79577e80a12d434d9b3b6e087b3a1d56
출처 데이터셋
uspto-grants-1977_04
특허 번호
US04017522

반응 노트

불러오는 중…