Dodecanoyl chloride → 2-[Benzoyl(2-dodecanoyloxyethyl)amino]ethyl dodecanoate

HRID 328428

반응식

HRID 328428 반응식
[OH:1][CH2:2][CH2:3][N:4]([CH2:13][CH2:14][OH:15])[C:5](=[O:12])[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1.[C:16](Cl)(=[O:28])[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH3:27]>>[C:16]([O:1][CH2:2][CH2:3][N:4]([CH2:13][CH2:14][O:15][C:16](=[O:28])[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH3:27])[C:5](=[O:12])[C:6]1[CH:7]=[CH:8][CH:9]=[CH:10][CH:11]=1)(=[O:28])[CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH3:27]

참가 물질

3

반응물 2

HCID 8166Dodecanoyl chlorideHCID 94109N,N-Bis(2-hydroxyethyl)benzamide

생성물 1

HCID 3216882-[Benzoyl(2-dodecanoyloxyethyl)amino]ethyl dodecanoate

실험 절차

N,N-bis(2-lauroyloxyethyl)-benzamide was prepared by the procedure of example 1 from 19.5 gms. (0.1 mole) of N,N-bis(2-hydroxyethyl)benzamide and 44 gms. (0.2 mole) of lauroyl chloride. The structure of the final product was characterized on the basis of IR and NMR spectral analyses as described in example 1.

후처리

  1. customN,N-bis(2-lauroyloxyethyl)-benzamide was prepared by the procedure of example 1 from 19.5 gms

출처 및 근거

ORD 기록
ord-ae27b68bebe9463b9370f4c75862162b
출처 데이터셋
uspto-grants-1977_04
특허 번호
US04017522

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