Dodecanoyl chloride → 2-[Methyl(4-methylbenzoyl)amino]ethyl dodecanoate

HRID 328443

반응식

HRID 328443 반응식
[CH3:1][N:2]([CH2:12][CH2:13][OH:14])[C:3]([C:5]1[CH:10]=[CH:9][C:8]([CH3:11])=[CH:7][CH:6]=1)=[O:4].[C:15](Cl)(=[O:27])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26]>>[CH3:1][N:2]([CH2:12][CH2:13][O:14][C:15](=[O:27])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH3:26])[C:3]([C:5]1[CH:10]=[CH:9][C:8]([CH3:11])=[CH:7][CH:6]=1)=[O:4]

참가 물질

3

반응물 2

HCID 8166Dodecanoyl chlorideHCID 21441887N-(2-hydroxyethyl)-N,4-dimethylbenzamide

생성물 1

HCID 214418812-[Methyl(4-methylbenzoyl)amino]ethyl dodecanoate

실험 절차

N-methyl-N-(2-lauroyloxyethyl)-p-toluamide was prepared by the procedure of example 1 from 19 gms. (0.1 mole) of N-methyl-N-(2-hydroxyethyl)-p-toluamide and 22 gms. (0.1 mole) of lauroyl chloride. The structure of the final product was characterized on the basis of IR and NMR spectral analyses as described in example 1.

후처리

  1. customN-methyl-N-(2-lauroyloxyethyl)-p-toluamide was prepared by the procedure of example 1 from 19 gms

출처 및 근거

ORD 기록
ord-18cfc6ff3a2249b884f95b49c1629176
출처 데이터셋
uspto-grants-1977_04
특허 번호
US04017522

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