Oleoyl chloride → N-methyl-N-(2-oleoyloxyethyl)-p-toluamide

HRID 328444

반응식

HRID 328444 반응식
[CH3:1][N:2]([CH2:12][CH2:13][OH:14])[C:3]([C:5]1[CH:10]=[CH:9][C:8]([CH3:11])=[CH:7][CH:6]=1)=[O:4].[C:15](Cl)(=[O:33])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22]/[CH:23]=[CH:24]\[CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32]>>[CH3:1][N:2]([CH2:12][CH2:13][O:14][C:15](=[O:33])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22]/[CH:23]=[CH:24]\[CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32])[C:3]([C:5]1[CH:10]=[CH:9][C:8]([CH3:11])=[CH:7][CH:6]=1)=[O:4]

참가 물질

3

반응물 2

HCID 5364783Oleoyl chlorideHCID 21441887N-(2-hydroxyethyl)-N,4-dimethylbenzamide

생성물 1

HCID 68123309N-methyl-N-(2-oleoyloxyethyl)-p-toluamide

실험 절차

N-methyl-N-(2-oleoyloxyethyl)-p-toluamide was prepared by the procedure of example 1 from 19 gms. (0.1 mole) of N-methyl-N-(2-hydroxyethyl)-p-toluamide and 30 gms. (0.1 mole) of oleoyl chloride. The structure of the final product was characterized on the basis of IR and NMR spectral analyses as described in example 1.

후처리

  1. customN-methyl-N-(2-oleoyloxyethyl)-p-toluamide was prepared by the procedure of example 1 from 19 gms

출처 및 근거

ORD 기록
ord-af13e5383dc24d6e8fc9b3614a7f2665
출처 데이터셋
uspto-grants-1977_04
특허 번호
US04017522

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