Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Miconazole → HCID 178521218, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Miconazole | HCID 4189 | — |
| 반응물 | 2,4-Dichloro-alpha-(chloromethyl)benzenemethanol | HCID 94351 | — |
| 용매 | Benzonitrile | HCID 7505 | — |
| 생성물 | HCID 178521218 | HCID 178521218 | — |
반응 단계
4.2 parts of 1-[2,4-dichloro-β-(2,4-dichlorobenzyloxy)-phenethyl]imidazole and 3 parts of 2,4-dichloro-α-(chloromethyl)-benzyl alcohol are mixed together in 40 parts of benzonitrile and the resulting mixture is stirred at reflux temperature for 3 days. At the end of this period the reaction solvent is evaporated off under reduced pressure to obtain a 1-[2,4-dichloro-β-(2,4-dichlorobenzyloxy)phenethyl]-3-(2,4-dichloro-β-hydroxyphenethyl)imidazolium chloride product as residue.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04017631 |
| 출처 데이터셋 | uspto-grants-1977_04 |
| ORD ID | ord-aaffdf9f544f4d1d8c883cf452d78b33 |
| 출처 메모 | uspto-grants-1977_04 |