Benzene → 3,4-dinitrobenzoyl Chloride

HRID 328746노트

반응식

HRID 328746 반응식
[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][C:12]=1[N+:13]([O-:15])=[O:14])[C:7](O)=[O:8])([O-:3])=[O:2].C1C=CC=CC=1.C(Cl)(=O)C([Cl:25])=O>N1C=CC=CC=1>[N+:1]([C:4]1[CH:5]=[C:6]([CH:10]=[CH:11][C:12]=1[N+:13]([O-:15])=[O:14])[C:7]([Cl:25])=[O:8])([O-:3])=[O:2]

참가 물질

5

반응물 3

HCID 241BenzeneHCID 107093,4-Dinitrobenzoic acidHCID 65578Oxalyl chloride

생성물 1

HCID 118064913,4-dinitrobenzoyl Chloride

시약·촉매·용매 1

HCID 1049Pyridine용매

실험 절차

Fifty-three grams (0.25 mole) of 3,4-dinitrobenzoic acid, 500 ml. of benzene, 65 g. (0.51 mole) of oxalyl chloride and 1 ml. of pyridine were reacted according to Example 2 (A), first paragraph, to provide 3,4-dinitrobenzoyl chloride as a crude oil.

출처 및 근거

ORD 기록
ord-839dba5eea18470c8312ecc4e251e62e
출처 데이터셋
uspto-grants-1977_04
특허 번호
US04018790

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