HCID 12408785, 화합물 → HCID 21440222, 화합물

반응식

[C:1]([C:9]1[C:17]([N+:18]([O-])=O)=[CH:16][C:12]([C:13]([OH:15])=[O:14])=[CH:11][C:10]=1[O:21][CH2:22][C:23]1C=CC=C[CH:24]=1)(=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.NC1C(C(=O)C2C=CC=CC=2)=C(OCCC)C=C(C=1)C(O)=O>>[NH2:18][C:17]1[C:9]([CH2:1][C:2]2[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=2)=[C:10]([O:21][CH2:22][CH2:23][CH3:24])[CH:11]=[C:12]([CH:16]=1)[C:13]([OH:15])=[O:14]

참가 물질

반응물 2

HCID 12408785HCID 12408785, 화합물

HCID 21440223HCID 21440223, 화합물

생성물 1

HCID 21440222HCID 21440222, 화합물

실험 절차

By replacing in Example 24, step A, 4-benzoyl-3-benzyloxy-5-nitrobenzoic acid with 5-amino-4-benzoyl-3-n-propoxybenzoic acid and following the procedure described, 5-amino-4-benzyl-3-n-propoxybenzoic acid is obtained with a melting point of 161°- 162° C.

출처 및 근거

ORD 기록: ord-8bb24bb0a267453ea2121f0a698ee0a2
출처 데이터셋: uspto-grants-1977_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04018794

반응 노트

불러오는 중…