HCID 21440117, 화합물 → HCID 21440173, 화합물

반응식

C(C1C([N+]([O-])=O)=CC(C(O)=O)=CC=1OCC1C=CC=CC=1)(=O)C1C=CC=CC=1.[NH2:29][C:30]1[C:31]([C:48](=O)[C:49]2[CH:54]=[CH:53][CH:52]=[CH:51][CH:50]=2)=[C:32]([O:39][CH2:40][C:41]2[CH:46]=[CH:45][C:44]([Cl:47])=[CH:43][CH:42]=2)[CH:33]=[C:34]([CH:38]=1)[C:35]([OH:37])=[O:36]>>[NH2:29][C:30]1[C:31]([CH2:48][C:49]2[CH:54]=[CH:53][CH:52]=[CH:51][CH:50]=2)=[C:32]([O:39][CH2:40][C:41]2[CH:46]=[CH:45][C:44]([Cl:47])=[CH:43][CH:42]=2)[CH:33]=[C:34]([CH:38]=1)[C:35]([OH:37])=[O:36]

참가 물질

반응물 2

HCID 21440117HCID 21440117, 화합물

HCID 21440223HCID 21440223, 화합물

생성물 1

HCID 21440173HCID 21440173, 화합물

실험 절차

By replacing in Example 24, step A, 4-benzoyl3-benzyloxy-5-nitrobenzoic acid with 5-amino-4-benzoyl-3-(p-chlorobenzyloxy)benzoic acid and following the procedure described, 5-amino-4-benzyl-3-(p-chlorobenzyloxy)benzoic acid is obtained with a melting point of 199°-200° C.

출처 및 근거

ORD 기록: ord-d5f808207d454dc6bfb71447a90262a0
출처 데이터셋: uspto-grants-1977_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04018794

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