Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methane → 2-(4-Heptyl-4-piperidyloxy)-ethanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methane | HCID 297 | — |
| 반응물 | 2-(1-Benzyl-4-heptyl-4-piperidyloxy)-ethanol | HCID 21440938 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 2-(4-Heptyl-4-piperidyloxy)-ethanol | HCID 21440901 | 36.3% |
반응 단계
A solution of 40 g of 2-(1-benzyl-4-heptyl-4-piperidyloxy)-ethanol in 300 ml of absolute ethanol was reacted with hydrogen at 50° C in the presence of 0.4 g of 5% palladized charcoal until the theoretical amount of hydrogen was absorbed and the catalyst was then filtered off. The ethanol was distilled off and the residue was rectified to obtain 10.6 g of 2-(4-heptyl-4-piperidyloxy)-ethanol as a colorless oil boiling at 110°-130° C at 0.1 mm Hg.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04018922 |
| 출처 데이터셋 | uspto-grants-1977_04 |
| ORD ID | ord-6f91d58563e24e39beddfffdeb6cce77 |
| 출처 메모 | uspto-grants-1977_04 |