Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetyl chloride → 1-(3-acetyltetrahydro-2H-1,3-thiazin-2-ylidene)-3-(2,4-dichlorophenoxy)-1-nitro-2-propanone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetyl chloride | HCID 6367 | — |
| 반응물 | Sodium hydride | HCID 24758 | — |
| 반응물 | 3-(2,4-dichlorophenoxy)-1-nitro-1-(tetrahydro-2H-1,3-thiazin-2-ylidene)-2-propanone | HCID 86734697 | — |
| 생성물 | 1-(3-acetyltetrahydro-2H-1,3-thiazin-2-ylidene)-3-(2,4-dichlorophenoxy)-1-nitro-2-propanone | HCID 54572089 | — |
반응 단계
5 was prepared as a yellow solid, melting point: 120°-120.5° (with decomposition) by the treatment of 5C with sodium hydride and acetyl chloride, by the general procedure described in Example 1.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04020061 |
| 출처 데이터셋 | uspto-grants-1977_04 |
| ORD ID | ord-acccc7e676614654bd37998f8b414146 |
| 출처 메모 | uspto-grants-1977_04 |