Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Azelaic Acid → Diprop-1-en-2-yl nonanedioate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Azelaic Acid | HCID 2266 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Diprop-1-en-2-yl nonanedioate | HCID 23466330 | — |
반응 단계
Azelaic acid (100 grams, 0.53 mole), methylene chloride (500 ml.) and mercuric acetate (18.2 grams, 0.057 mole) are treated with 1 ml. of boron trifluoride etherate, and propyne gas is bubbled through the mixture for 3 hours. Solid sodium bicarbonate (5 grams) is added, and the mixture is filtered free of solids and metallic mercury.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04020123 |
| 출처 데이터셋 | uspto-grants-1977_04 |
| ORD ID | ord-7e0bf1f8d03f4384b7b8d833b3bfe3a2 |
| 출처 메모 | uspto-grants-1977_04 |