참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 1,1,3,3-Tetramethyl-disiloxane | HCID 18659 | — |
| 반응물 | N-Allylcyclohexylamine | HCID 81115 | — |
| 촉매 | Chloroplatinic acid | HCID 61859 | — |
| 생성물 | 1,3-bis(N-cyclohexyl-3-aminopropyl)-1,1,3,3-tetramethyldisiloxane | HCID 19871404 | — |
반응 단계
Following the technique described in Example 1, N-allylcyclohexylamine (0.173 mole), 1,1,3,3-tetramethyldisiloxane (0.0783 mole), and 0.05 g hexachloroplatinic acid are stirred at 70° C for eight hours at 110° C. under nitrogen. The product, in nearly quantitative yield, is purified by vacuum distillation at <1 torr at a temperature of 207°-210° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04892918 |
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| 출처 데이터셋 | uspto-grants-1990_01 |
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| ORD ID | ord-c0289677df37416ba173f315dea44ca7 |
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| 출처 메모 | uspto-grants-1990_01 |
|---|
