Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Perchlorate → Phenylphosphine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Perchlorate | HCID 123351 | — |
| 반응물 | 1-Methylphenylphosphanium carbonate | HCID 86743659 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Phenylphosphine | HCID 12519 | — |
| 생성물 | Methylphosphanium perchlorate | HCID 19871530 | — |
반응 단계
By following the same procedure as the 2nd step of Example 12 except that 10.0 g of 1-methylphenylphosphanium carbonate, 6.9 g of 60% perchlorate, and 10.0 g of water were used, 10.9 g (94.8% of the theoretical yield, yield of 67.6% to 1-phenylphosphane) of methylphosphanium perchlorate was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04892944 |
| 출처 데이터셋 | uspto-grants-1990_01 |
| ORD ID | ord-f1dfed6d36574850a6245e0f377c767f |
| 출처 메모 | uspto-grants-1990_01 |