참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 1-(4-Chlorophenyl)-1-octen-3-one | HCID 54522967 | — |
| 촉매 | Nickel | HCID 935 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 1-(4-Chlorophenyl)-3-octanone | HCID 14537610 | 96.4% |
반응 단계
15 g of Raney nickel are added to a solution of 100 g (0.423 mol) of 1-(4-chlorophenyl)-1-octen-3-one in 500 ml of toluene and the mixture is stirred for 5 hours at 60° C. under a hydrogen pressure of 70-90 bar in an autoclave. After this the reaction mixture is filtered and concentrated under reduced pressure. 97.3 g (96.4% of theory) of 1-(4-chlorophenyl)-3-octanone are obtained in the form of a colorless oil. ##STR36##
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04894383 |
|---|
| 출처 데이터셋 | uspto-grants-1990_01 |
|---|
| ORD ID | ord-e5bf4d7c678448c0b877ea636881a094 |
|---|
| 출처 메모 | uspto-grants-1990_01 |
|---|
