Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → HCID 178511167, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Formaldehyde | HCID 712 | — |
| 반응물 | Phosphorous acid | HCID 107909 | — |
| 반응물 | 2-Hydroxyputrescine | HCID 164656 | — |
| 생성물 | HCID 178511167 | HCID 178511167 | — |
반응 단계
To a 500 ml three neck flask fitted with a reflux condenser and dropping funnel is added 131.2 grams (1.12 moles) 70% phosphorous acid and 207.2 grams (2.1 moles) 37% hydrochloric acid. Aminoethyl ethanolamine, 42.1 grams (0.40 mole) is then added dropwise while stirring. The mixture is then heated to reflux and 97.3 grams (1.2 moles) 37% aqueous formaldehyde is added dropwise during 1 hour. Reflux is continued for 2 hours after completion of the formaldehyde addition. The mixture is then cooled and bottled.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04895600 |
| 출처 데이터셋 | uspto-grants-1990_01 |
| ORD ID | ord-f5e410aebe704cc896a775c07499a96a |
| 출처 메모 | uspto-grants-1990_01 |