Dichloromethane → HCID 85556110, 화합물

반응식

C([NH:8][CH2:9][CH:10]([CH2:12][S:13][CH:14]([CH3:16])[CH3:15])[OH:11])(OC(C)(C)C)=O.C(Cl)[Cl:18]>>[NH2:8][CH2:9][CH:10]([CH2:12][S:13][CH:14]([CH3:16])[CH3:15])[OH:11].[ClH:18]

참가 물질

반응물 2

HCID 6344Dichloromethane

HCID 131716253HCID 131716253, 화합물

생성물 1

HCID 85556110HCID 85556110, 화합물

실험 절차

BOC-NHCH2CH(OH)CH2SCH(CH3)2 (3.74 g, 0.015 mole) was dissolved in 75 ml CH2Cl2 and occasionally purged with HCl gas over two hours. The solvent was removed in vacuo, and the residue was triturated with Et2O. The solvent was decanted and the residue was stripped to a foam, 2.83 g. IR, NMR, and mass spectral analysis confirmed the structure.

후처리

customoccasionally purged with HCl gas over two hours
customThe solvent was removed in vacuo
customthe residue was triturated with Et2O
customThe solvent was decanted

출처 및 근거

ORD 기록: ord-d9dac2abfee148078775f620edc16bb6
출처 데이터셋: uspto-grants-1990_01
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04895834

반응 노트

불러오는 중…