Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Toluene → Allylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Toluene | HCID 1140 | — |
| 반응물 | Triethoxysilane | HCID 13830 | — |
| 반응물 | Trimethoxysilane | HCID 17215 | — |
| 반응물 | Aminopropyltrimethoxysilane | HCID 83756 | — |
| 용매 | P-Xylene | HCID 7809 | — |
| 생성물 | Allylamine | HCID 7853 | — |
| 생성물 | Trimethoxysilane | HCID 17215 | — |
반응 단계
Example 1 was repeated except that the 41 grams of triethoxy silane was replaced with 30.6 grams of trimethoxy silane (0.25 mole) and toluene was used as a solvent instead of p-xylene, with other conditions remaining the same. After the completion of the reaction, the reaction mixture was subjected to gas chromatography analysis. It was found that gamma-aminopropyl trimethoxy silane was obtained in a yield of 70% on an allylamine basis, while the yield of beta-amminopropyl trimethoxy silane was 0.9% on an a trimethoxy silane basis.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04897501 |
| 출처 데이터셋 | uspto-grants-1990_01 |
| ORD ID | ord-e3577c4eabb146a69b54c6f965de7145 |
| 출처 메모 | uspto-grants-1990_01 |