참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Butyl isocyanate | HCID 8110 | — |
| 반응물 | N,N',N''-Tris(3-dimethylaminopropyl)hexahydro-S-triazine | HCID 85160 | — |
| 반응물 | Isocyanate | HCID 105034 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Carbamic acid, N-butyl-, ethyl ester | HCID 11577 | — |
반응 단계
In a 250 ml round-bottomed flask, 0.02 g of Desmorapid Z, 34.1 g of n-butyl isocyanate were initially introduced and heated to 60° C. Thereafter, 15.9 g of ethanol were added dropwise and the mixture was further kept at 60° C. until the isocyanate content had fallen below 0.1%. Thereafter, cooling was effected and the product was obtained as a clear liquid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08877408B2 |
|---|
| 출처 데이터셋 | uspto-grants-2014_11 |
|---|
| ORD ID | ord-539659cc286943089e7eb0f073eca70f |
|---|
| 출처 메모 | uspto-grants-2014_11 |
|---|
