Tetrafluoro-m-phenylenediamine dihydrochloride → n-(2-Pyrid-2-ylethyl)benzene-1,4-diamine dihydrochloride
반응식
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([NH:10][CH2:11][CH2:12][C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][N:14]=2)=[CH:6][CH:5]=1)([O-])=O.C1(N)C(F)=C(F)C(F)=C(N)C=1F.[ClH:31].Cl>[Zn].[Cl-].[NH4+].O.C(O)C>[ClH:31].[ClH:31].[N:14]1[CH:15]=[CH:16][CH:17]=[CH:18][C:13]=1[CH2:12][CH2:11][NH:10][C:7]1[CH:6]=[CH:5][C:4]([NH2:1])=[CH:9][CH:8]=1참가 물질
4
실험 절차
The N-(4-nitrophenyl)-N-(2-pyrid-2-ylethyl)amine (5) obtained above was reduced with a boiling zinc/ammonium chloride/water/ethanol mixture. The corresponding amine was isolated in dihydrochloride form.
출처 및 근거
- ORD 기록
- ord-fe6fe9f925824fb6aea92d62733bbd4f
- 출처 데이터셋
- uspto-grants-2008_09
- 특허 번호
- US07429278B2
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