Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Azobisisobutyronitrile → 2-Bromoindenone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Azobisisobutyronitrile | HCID 6547 | — |
| 반응물 | N-bromobutanimide | HCID 67184 | — |
| 반응물 | 1H-inden-1-one | HCID 11815384 | — |
| 용매 | Carbon Tetrachloride | HCID 5943 | — |
| 생성물 | 2-Bromoindenone | HCID 9990649 | — |
반응 단계
The indenone compound of formula 16 prepared in Step 3 is dissolved in CCl4, N-bromosuccinimide (1 to 1.2 eq) and 2,2′-azobisisobutyronitrile (10 to 15 wt %) are added thereto. The resulting mixture is allowed to reflux for 2 to 3 h with stirring, to obtain the 2-bromoindenone of formula 17.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08877747B2 |
| 출처 데이터셋 | uspto-grants-2014_11 |
| ORD ID | ord-fd65a78cb4b1405d8b8fc847e893edc2 |
| 출처 메모 | uspto-grants-2014_11 |