Bromine → 2-Bromoindenone

HRID 331258

반응식

HRID 331258 반응식
[C:1]1(=[O:10])[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[CH:3]=[CH:2]1.[Br:11]Br>C(Cl)Cl>[Br:11][C:2]1[C:1](=[O:10])[C:9]2[C:4]([CH:3]=1)=[CH:5][CH:6]=[CH:7][CH:8]=2

참가 물질

4

반응물 2

HCID 24408BromineHCID 118153841H-inden-1-one

생성물 1

HCID 99906492-Bromoindenone

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

The indenone of formula 23 prepared in Step 2 is dissolved in CH2Cl2, 1M Br2 solution (dissolved in CH2Cl2) is added thereto. The resulting mixture is stirred for 2 to 3 h at room temperature, to obtain the 2-bromoindenone of formula 17.

출처 및 근거

ORD 기록
ord-16453f5f62194f7e87fa552a871847dd
출처 데이터셋
uspto-grants-2014_11
특허 번호
US08877747B2

연결된 노트

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