Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → HCID 67204923, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | Piperidine | HCID 8082 | — |
| 반응물 | (Z)-3-((1H-pyrrol-2-yl)methylene)indolin-2-one | HCID 5908088 | — |
| 반응물 | HCID 15956689 | HCID 15956689 | — |
| 생성물 | HCID 67204923 | HCID 67204923 | 81% |
반응 단계
To a stirred solution of oxindole 1 (4.19 g, 25 mmol) in methanol (50 mL) was added aldehyde 2 (3.96 g, 25 mmol) and piperidine (2.45 mL, 25 mmol). The reaction mixture was stirred at room temperature for 3 h and the yellow precipitate was collected, washed successively with methanol, hexanes, and ethyl ether and dried to give compound 3 (6.25 g, 81% yield).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08877796B2 |
| 출처 데이터셋 | uspto-grants-2014_11 |
| ORD ID | ord-f7e546787b0b48b78a554e039112702f |
| 출처 메모 | uspto-grants-2014_11 |