Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Trimethylsilyldiazomethane → Methyl 5-formylfuran-2-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Trimethylsilyldiazomethane | HCID 167693 | — |
| 반응물 | 5-Formyl-2-furancarboxylic Acid | HCID 2793719 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | Methyl 5-formylfuran-2-carboxylate | HCID 12283779 | — |
반응 단계
5-Formyl-2-furancarboxylic acid (5 g, 35.7 mmol) was dissolved in acetone (100 mL), and trimethylsilyl-diazomethane/2M hexane solution (23.2 mL, 46.4 mmol) was slowly added dropwise at room temperature. After stirring at room temperature for 10 minutes, the solvent was evaporated under reduced pressure to give 5-formyl-2-furancarboxylic acid methyl ester as a crude product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08877805B2 |
| 출처 데이터셋 | uspto-grants-2014_11 |
| ORD ID | ord-f7bcdd8ed3a44b75afc4740aea08f9ad |
| 출처 메모 | uspto-grants-2014_11 |