Acetic Acid → Tetraethylammonium acetate

반응식

[OH-].[CH2:2]([N+:4]([CH2:9][CH3:10])([CH2:7][CH3:8])[CH2:5][CH3:6])[CH3:3].[C:11]([OH:14])(=[O:13])[CH3:12]>>[C:11]([O-:14])(=[O:13])[CH3:12].[CH2:2]([N+:4]([CH2:9][CH3:10])([CH2:7][CH3:8])[CH2:5][CH3:6])[CH3:3]

참가 물질

반응물 2

HCID 176Acetic Acid

HCID 6509Tetraethylammonium Hydroxide

생성물 1

HCID 102017Tetraethylammonium acetate

실험 절차

Into an eggplant-shaped flask, an aqueous tetraethylammonium hydroxide solution (1 mol) was charged, and while it was cooled to maintain room temperature, acetic acid (1 mol) was added to obtain tetraethylammonium acetate. Then, ethylene glycol was added as a solvent so that it became a predetermined concentration, and by means of an evaporator, water was distilled off to obtain a solution comprising 50% of tetraethylammonium acetate and 50% of ethylene glycol.

후처리

temperaturewhile it was cooled

출처 및 근거

ORD 기록: ord-c1fbea0ea0e64df0a323060c542a36b5
출처 데이터셋: uspto-grants-2014_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08877825B2

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