Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzylamine → GlyTouCan:G63996AI
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzylamine | HCID 7504 | — |
| 반응물 | beta-D-Galactose pentaacetate | HCID 94752 | — |
| 용매 | Tetrahydrofuran | HCID 8028 | — |
| 생성물 | GlyTouCan:G63996AI | HCID 11152232 | — |
반응 단계
The synthesis of compound 9 is illustrated in FIG. 6. 20 g (51.24 mmol) of β-D-galactosepentaacetate 1 was dissolved in 150 ml THF and 6.7 ml (61.49 mmol) of benzylamine was added with a dropping funnel. The reaction was stirred for 18 h at room temperature to give 2,3,4,6-tetra-O-acetyl-β-D-galactopyranose 2.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08877917B2 |
| 출처 데이터셋 | uspto-grants-2014_11 |
| ORD ID | ord-9208ea680a3d4041996f1373e850ba66 |
| 출처 메모 | uspto-grants-2014_11 |